data_roberta1
_audit_creation_date              2015-03-05
_audit_creation_method
;
Olex2 1.2
(compiled 2015.01.26 svn.r3150 for OlexSys, GUI svn.r4998)
;
_publ_contact_author_address      ?
_publ_contact_author_email        ?
_publ_contact_author_name         ''
_publ_contact_author_phone        ?
_publ_section_references
;
Dolomanov, O.V., Bourhis, L.J., Gildea, R.J, Howard, J.A.K. & Puschmann, H.
 (2009), J. Appl. Cryst. 42, 339-341.

Sheldrick, G.M. (2008). Acta Cryst. A64, 112-122.
;
_chemical_name_common             ?
_chemical_name_systematic
;
 ? 
;
_chemical_formula_moiety          'C12 H20 Cl2 N Rh'
_chemical_formula_sum             'C12 H20 Cl2 N Rh'
_chemical_formula_weight          352.10
_chemical_melting_point           ?
loop_
  _atom_type_symbol
  _atom_type_description
  _atom_type_scat_dispersion_real
  _atom_type_scat_dispersion_imag
  _atom_type_scat_source
 'C' 'C' 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
 'H' 'H' 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
 'Cl' 'Cl' 0.1484 0.1585 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
 'N' 'N' 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
 'Rh' 'Rh' -1.1178 0.9187
 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'

_space_group_crystal_system       'monoclinic'
_space_group_IT_number            14
_space_group_name_H-M_alt         'P 21/n'
_space_group_name_Hall            '-P 2yn'
loop_
  _space_group_symop_id
  _space_group_symop_operation_xyz
 1 'x, y, z'
 2 '-x+1/2, y+1/2, -z+1/2'
 3 '-x, -y, -z'
 4 'x-1/2, -y-1/2, z-1/2'

_cell_length_a                    8.3712(7)
_cell_length_b                    9.2289(7)
_cell_length_c                    18.9787(16)
_cell_angle_alpha                 90.00
_cell_angle_beta                  99.136(4)
_cell_angle_gamma                 90.00
_cell_volume                      1447.6(2)
_cell_formula_units_Z             4
_cell_measurement_reflns_used     ?
_cell_measurement_temperature     173(2)
_cell_measurement_theta_max       ?
_cell_measurement_theta_min       ?
_exptl_absorpt_coefficient_mu     1.524
_exptl_absorpt_correction_T_max   0.7460
_exptl_absorpt_correction_T_min   0.6582
_exptl_absorpt_correction_type    multi-scan
_exptl_absorpt_process_details
;
SADABS-2012/1 (Bruker,2012) was used for absorption correction.
wR2(int) was 0.0468 before and 0.0357 after correction.
The Ratio of minimum to maximum transmission is 0.8823.
The \l/2 correction factor is 0.0015.
;
_exptl_crystal_colour             orange
_exptl_crystal_colour_primary     orange
_exptl_crystal_density_diffrn     1.616
_exptl_crystal_density_meas       ?
_exptl_crystal_density_method     'not measured'
_exptl_crystal_description        irregular
_exptl_crystal_F_000              712
_exptl_crystal_preparation        ?
_exptl_crystal_size_max           0.25
_exptl_crystal_size_mid           0.21
_exptl_crystal_size_min           0.19
_exptl_special_details
;
 ? 
;
_diffrn_reflns_av_R_equivalents   0.0206
_diffrn_reflns_av_unetI/netI      0.0188
_diffrn_reflns_limit_h_max        11
_diffrn_reflns_limit_h_min        -11
_diffrn_reflns_limit_k_max        12
_diffrn_reflns_limit_k_min        -12
_diffrn_reflns_limit_l_max        26
_diffrn_reflns_limit_l_min        -23
_diffrn_reflns_number             15249
_diffrn_reflns_theta_full         29.79
_diffrn_reflns_theta_max          29.79
_diffrn_reflns_theta_min          2.17
_diffrn_ambient_temperature       173.15
_diffrn_detector_area_resol_mean  'Rotation images'
_diffrn_measured_fraction_theta_full 0.992
_diffrn_measured_fraction_theta_max 0.992
_diffrn_measurement_device_type   'Bruker X8 Apex diffractometer'
_diffrn_measurement_method        'Rotation images'
_diffrn_radiation_monochromator   graphite
_diffrn_radiation_type            MoK\a
_diffrn_radiation_wavelength      0.71073
_diffrn_source                    'fine-focus sealed tube'
_diffrn_standards_decay_%         0
_diffrn_standards_interval_count  0
_diffrn_standards_interval_time   0
_diffrn_standards_number          0
_reflns_number_gt                 3758
_reflns_number_total              4111
_reflns_threshold_expression      >2sigma(I)
_computing_cell_refinement        'APEX 2 software, Bruker Nonius 2004'
_computing_data_collection        'APEX 2 software, Bruker Nonius 2004'
_computing_data_reduction         'SAINT, Bruker Nonius 2004'
_computing_molecular_graphics     'Olex2 (Dolomanov et al., 2009)'
_computing_publication_material   'Olex2 (Dolomanov et al., 2009)'
_computing_structure_refinement   'ShelXL (Sheldrick, 2008)'
_computing_structure_solution     'SHELXS-97 (Sheldrick, 1990)'
_refine_diff_density_max          1.846
_refine_diff_density_min          -0.855
_refine_diff_density_rms          0.097
_refine_ls_extinction_coef        ?
_refine_ls_extinction_method      none
_refine_ls_goodness_of_fit_ref    1.043
_refine_ls_hydrogen_treatment     constr
_refine_ls_matrix_type            full
_refine_ls_number_parameters      145
_refine_ls_number_reflns          4111
_refine_ls_number_restraints      0
_refine_ls_R_factor_all           0.0399
_refine_ls_R_factor_gt            0.0364
_refine_ls_restrained_S_all       1.043
_refine_ls_shift/su_max           0.000
_refine_ls_shift/su_mean          0.000
_refine_ls_structure_factor_coef  Fsqd
_refine_ls_weighting_details
'calc w=1/[\s^2^(Fo^2^)+(0.0473P)^2^+2.3401P] where P=(Fo^2^+2Fc^2^)/3'
_refine_ls_weighting_scheme       calc
_refine_ls_wR_factor_gt           0.0946
_refine_ls_wR_factor_ref          0.0971
_refine_special_details
;
 Refinement of F^2^ against ALL reflections.  The weighted R-factor wR and 
 goodness of fit S are based on F^2^, conventional R-factors R are based 
 on F, with F set to zero for negative F^2^. The threshold expression of 
 F^2^ > 2sigma(F^2^) is used only for calculating R-factors(gt) etc. and is 
 not relevant to the choice of reflections for refinement.  R-factors based 
 on F^2^ are statistically about twice as large as those based on F, and R- 
 factors based on ALL data will be even larger. 
;
_olex2_refinement_description
;
1. Fixed Uiso
 At 1.2 times of:
  All C(H,H) groups, All N(H,H) groups
 At 1.5 times of:
  All C(H,H,H) groups
2.a Secondary CH2 refined with riding coordinates:
 N1(H1A,H1B), C10(H10A,H10B), C11(H11A,H11B), C12(H12A,H12B)
2.b Me refined with riding coordinates:
 C6(H6A,H6B,H6C), C7(H7A,H7B,H7C), C8(H8A,H8B,H8C), C9(H9A,H9B,H9C)
;
_atom_sites_solution_hydrogens    geom
_atom_sites_solution_primary      direct
_atom_sites_solution_secondary    difmap
loop_
  _atom_site_label
  _atom_site_type_symbol
  _atom_site_fract_x
  _atom_site_fract_y
  _atom_site_fract_z
  _atom_site_U_iso_or_equiv
  _atom_site_adp_type
  _atom_site_occupancy
  _atom_site_calc_flag
  _atom_site_disorder_assembly
  _atom_site_disorder_group
  _atom_site_refinement_flags_posn
 H1A H 0.9279 0.1386 -0.0164 0.055 Uiso 1 calc . . R
 H1B H 0.8192 0.0299 0.0081 0.055 Uiso 1 calc . . R
 C1 C 0.7461(4) 0.3352(3) 0.12632(15) 0.0341(6) Uani 1 d . . .
 C2 C 0.9023(5) 0.4085(3) 0.1365(2) 0.0462(8) Uani 1 d . . .
 C3 C 0.9997(4) 0.3457(4) 0.2002(2) 0.0481(8) Uani 1 d . . .
 C4 C 0.9071(4) 0.2376(4) 0.22765(16) 0.0407(6) Uani 1 d . . .
 C5 C 0.7508(3) 0.2291(3) 0.18216(15) 0.0343(5) Uani 1 d . . .
 C6 C 0.9499(8) 0.5330(5) 0.0938(3) 0.090(2) Uani 1 d . . .
 C7 C 1.1683(5) 0.3934(6) 0.2311(3) 0.0885(19) Uani 1 d . . .
 C8 C 0.9537(7) 0.1451(6) 0.2941(2) 0.0745(13) Uani 1 d . . .
 C9 C 0.6131(5) 0.1332(5) 0.1967(2) 0.0609(10) Uani 1 d . . .
 C10 C 0.6037(5) 0.3598(5) 0.0675(2) 0.0562(10) Uani 1 d . . .
 C11 C 0.5712(5) 0.2335(7) 0.0109(2) 0.0755(14) Uani 1 d . . .
 C12 C 0.7009(6) 0.2047(6) -0.0306(2) 0.0699(13) Uani 1 d . . .
 N1 N 0.8440(3) 0.1270(3) 0.00913(15) 0.0457(6) Uani 1 d . . .
 Cl1 Cl 0.94938(16) -0.07870(10) 0.13822(6) 0.0705(3) Uani 1 d . . .
 Cl2 Cl 1.19805(11) 0.19017(14) 0.07842(7) 0.0742(4) Uani 1 d . . .
 Rh1 Rh 0.93428(2) 0.18211(2) 0.117650(12) 0.03173(8) Uani 1 d . . .

loop_
  _atom_site_aniso_label
  _atom_site_aniso_U_11
  _atom_site_aniso_U_22
  _atom_site_aniso_U_33
  _atom_site_aniso_U_23
  _atom_site_aniso_U_13
  _atom_site_aniso_U_12
 C1 0.0399(15) 0.0310(12) 0.0337(13) -0.0008(10) 0.0128(11) 0.0097(11)
 C2 0.062(2) 0.0275(13) 0.0573(19) -0.0134(13) 0.0358(17) -0.0104(13)
 C3 0.0377(16) 0.0531(18) 0.0555(19) -0.0310(16) 0.0138(14) -0.0070(14)
 C4 0.0420(16) 0.0436(16) 0.0349(14) -0.0082(12) 0.0015(12) 0.0065(13)
 C5 0.0323(13) 0.0381(14) 0.0334(13) 0.0037(11) 0.0074(10) 0.0003(11)
 C6 0.159(6) 0.039(2) 0.093(3) -0.012(2) 0.080(4) -0.032(3)
 C7 0.043(2) 0.114(4) 0.109(4) -0.072(4) 0.012(2) -0.023(2)
 C8 0.091(3) 0.085(3) 0.0405(19) 0.007(2) -0.009(2) 0.018(3)
 C9 0.057(2) 0.074(3) 0.055(2) 0.0082(19) 0.0206(17) -0.022(2)
 C10 0.058(2) 0.064(2) 0.0460(18) 0.0043(16) 0.0045(15) 0.0346(19)
 C11 0.050(2) 0.118(4) 0.053(2) -0.007(3) -0.0072(18) 0.025(3)
 C12 0.061(3) 0.091(3) 0.051(2) -0.016(2) -0.0108(18) 0.027(2)
 N1 0.0383(14) 0.0519(16) 0.0443(14) -0.0165(12) -0.0018(11) 0.0113(12)
 Cl1 0.1055(9) 0.0343(4) 0.0677(6) -0.0042(4) 0.0012(6) 0.0190(5)
 Cl2 0.0306(4) 0.1049(9) 0.0902(8) -0.0591(7) 0.0191(4) -0.0099(4)
 Rh1 0.02519(12) 0.03090(12) 0.03809(13) -0.01081(8) 0.00190(8) 0.00244(7)

_geom_special_details
;
 All esds (except the esd in the dihedral angle between two l.s. planes) 
 are estimated using the full covariance matrix.  The cell esds are taken 
 into account individually in the estimation of esds in distances, angles 
 and torsion angles; correlations between esds in cell parameters are only 
 used when they are defined by crystal symmetry.  An approximate (isotropic) 
 treatment of cell esds is used for estimating esds involving l.s. planes. 
;
loop_
  _geom_bond_atom_site_label_1
  _geom_bond_atom_site_label_2
  _geom_bond_distance
  _geom_bond_site_symmetry_2
  _geom_bond_publ_flag
 C1 C2 1.457(5) . ?
 C1 C5 1.438(4) . ?
 C1 C10 1.515(5) . ?
 C2 C3 1.466(6) . ?
 C2 C6 1.496(5) . ?
 C3 C4 1.413(5) . ?
 C3 C7 1.506(5) . ?
 C4 C5 1.451(4) . ?
 C4 C8 1.522(5) . ?
 C5 C9 1.513(4) . ?
 C10 C11 1.580(7) . ?
 C11 C12 1.463(6) . ?
 N1 H1A 0.9200 . ?
 N1 H1B 0.9200 . ?
 N1 C12 1.494(5) . ?
 Rh1 C1 2.141(3) . ?
 Rh1 C2 2.143(3) . ?
 Rh1 C3 2.181(3) . ?
 Rh1 C4 2.196(3) . ?
 Rh1 C5 2.155(3) . ?
 Rh1 N1 2.139(3) . ?
 Rh1 Cl1 2.4386(10) . ?
 Rh1 Cl2 2.4408(9) . ?

loop_
  _geom_angle_atom_site_label_1
  _geom_angle_atom_site_label_2
  _geom_angle_atom_site_label_3
  _geom_angle
  _geom_angle_site_symmetry_1
  _geom_angle_site_symmetry_3
  _geom_angle_publ_flag
 C2 C1 C10 127.7(3) . . ?
 C2 C1 Rh1 70.19(17) . . ?
 C5 C1 C2 107.4(3) . . ?
 C5 C1 C10 124.8(3) . . ?
 C5 C1 Rh1 70.95(16) . . ?
 C10 C1 Rh1 123.0(2) . . ?
 C1 C2 C3 107.2(3) . . ?
 C1 C2 C6 126.6(4) . . ?
 C1 C2 Rh1 70.04(15) . . ?
 C3 C2 C6 126.1(4) . . ?
 C3 C2 Rh1 71.60(18) . . ?
 C6 C2 Rh1 127.4(3) . . ?
 C2 C3 C7 124.7(4) . . ?
 C2 C3 Rh1 68.80(17) . . ?
 C4 C3 C2 108.5(3) . . ?
 C4 C3 C7 126.7(4) . . ?
 C4 C3 Rh1 71.74(17) . . ?
 C7 C3 Rh1 126.5(2) . . ?
 C3 C4 C5 108.3(3) . . ?
 C3 C4 C8 128.2(4) . . ?
 C3 C4 Rh1 70.61(18) . . ?
 C5 C4 C8 123.5(3) . . ?
 C5 C4 Rh1 69.00(16) . . ?
 C8 C4 Rh1 127.3(3) . . ?
 C1 C5 C4 108.5(3) . . ?
 C1 C5 C9 126.9(3) . . ?
 C1 C5 Rh1 69.93(15) . . ?
 C4 C5 C9 124.4(3) . . ?
 C4 C5 Rh1 72.06(17) . . ?
 C9 C5 Rh1 128.2(3) . . ?
 C1 C10 C11 114.9(3) . . ?
 C12 C11 C10 115.9(4) . . ?
 C11 C12 N1 114.8(4) . . ?
 H1A N1 H1B 106.9 . . ?
 C12 N1 H1A 107.3 . . ?
 C12 N1 H1B 107.3 . . ?
 C12 N1 Rh1 120.3(2) . . ?
 Rh1 N1 H1A 107.3 . . ?
 Rh1 N1 H1B 107.3 . . ?
 C1 Rh1 C2 39.77(13) . . ?
 C1 Rh1 C3 65.93(13) . . ?
 C1 Rh1 C4 65.45(11) . . ?
 C1 Rh1 C5 39.11(11) . . ?
 C1 Rh1 Cl1 131.21(9) . . ?
 C1 Rh1 Cl2 135.68(9) . . ?
 C2 Rh1 C3 39.61(15) . . ?
 C2 Rh1 C4 65.13(13) . . ?
 C2 Rh1 C5 65.78(11) . . ?
 C2 Rh1 Cl1 160.05(10) . . ?
 C2 Rh1 Cl2 99.46(9) . . ?
 C3 Rh1 C4 37.65(13) . . ?
 C3 Rh1 Cl1 124.56(12) . . ?
 C3 Rh1 Cl2 93.55(9) . . ?
 C4 Rh1 Cl1 95.08(9) . . ?
 C4 Rh1 Cl2 121.21(9) . . ?
 C5 Rh1 C3 64.72(12) . . ?
 C5 Rh1 C4 38.94(11) . . ?
 C5 Rh1 Cl1 97.54(9) . . ?
 C5 Rh1 Cl2 158.15(8) . . ?
 N1 Rh1 C1 94.53(11) . . ?
 N1 Rh1 C2 110.97(13) . . ?
 N1 Rh1 C3 149.95(14) . . ?
 N1 Rh1 C4 153.70(12) . . ?
 N1 Rh1 C5 114.84(11) . . ?
 N1 Rh1 Cl1 85.47(9) . . ?
 N1 Rh1 Cl2 84.94(8) . . ?
 Cl1 Rh1 Cl2 93.01(5) . . ?

loop_
  _geom_torsion_atom_site_label_1
  _geom_torsion_atom_site_label_2
  _geom_torsion_atom_site_label_3
  _geom_torsion_atom_site_label_4
  _geom_torsion
  _geom_torsion_site_symmetry_1
  _geom_torsion_site_symmetry_2
  _geom_torsion_site_symmetry_3
  _geom_torsion_site_symmetry_4
  _geom_torsion_publ_flag
 C1 C2 C3 C4 0.3(3) . . . . ?
 C1 C2 C3 C7 -178.2(3) . . . . ?
 C1 C2 C3 Rh1 61.35(19) . . . . ?
 C1 C10 C11 C12 -62.3(6) . . . . ?
 C1 Rh1 C2 C3 116.9(3) . . . . ?
 C1 Rh1 C2 C6 -121.3(5) . . . . ?
 C1 Rh1 C3 C2 -38.68(18) . . . . ?
 C1 Rh1 C3 C4 80.5(2) . . . . ?
 C1 Rh1 C3 C7 -156.9(5) . . . . ?
 C1 Rh1 C4 C3 -81.8(2) . . . . ?
 C1 Rh1 C4 C5 37.63(17) . . . . ?
 C1 Rh1 C4 C8 154.4(4) . . . . ?
 C1 Rh1 C5 C4 -118.3(3) . . . . ?
 C1 Rh1 C5 C9 121.7(4) . . . . ?
 C1 Rh1 N1 C12 4.2(4) . . . . ?
 C2 C1 C5 C4 1.0(3) . . . . ?
 C2 C1 C5 C9 175.7(3) . . . . ?
 C2 C1 C5 Rh1 -61.05(19) . . . . ?
 C2 C1 C10 C11 108.7(4) . . . . ?
 C2 C3 C4 C5 0.3(3) . . . . ?
 C2 C3 C4 C8 -178.1(3) . . . . ?
 C2 C3 C4 Rh1 59.2(2) . . . . ?
 C2 Rh1 C1 C5 -117.5(3) . . . . ?
 C2 Rh1 C1 C10 122.8(4) . . . . ?
 C2 Rh1 C3 C4 119.1(3) . . . . ?
 C2 Rh1 C3 C7 -118.2(5) . . . . ?
 C2 Rh1 C4 C3 -37.9(2) . . . . ?
 C2 Rh1 C4 C5 81.6(2) . . . . ?
 C2 Rh1 C4 C8 -161.6(4) . . . . ?
 C2 Rh1 C5 C1 38.50(19) . . . . ?
 C2 Rh1 C5 C4 -79.8(2) . . . . ?
 C2 Rh1 C5 C9 160.2(3) . . . . ?
 C2 Rh1 N1 C12 -33.1(4) . . . . ?
 C3 C4 C5 C1 -0.8(3) . . . . ?
 C3 C4 C5 C9 -175.7(3) . . . . ?
 C3 C4 C5 Rh1 59.9(2) . . . . ?
 C3 Rh1 C1 C2 38.5(2) . . . . ?
 C3 Rh1 C1 C5 -78.9(2) . . . . ?
 C3 Rh1 C1 C10 161.3(3) . . . . ?
 C3 Rh1 C2 C1 -116.9(3) . . . . ?
 C3 Rh1 C2 C6 121.8(5) . . . . ?
 C3 Rh1 C4 C5 119.5(3) . . . . ?
 C3 Rh1 C4 C8 -123.8(4) . . . . ?
 C3 Rh1 C5 C1 82.3(2) . . . . ?
 C3 Rh1 C5 C4 -36.0(2) . . . . ?
 C3 Rh1 C5 C9 -156.0(3) . . . . ?
 C3 Rh1 N1 C12 -42.9(5) . . . . ?
 C4 Rh1 C1 C2 80.0(2) . . . . ?
 C4 Rh1 C1 C5 -37.47(18) . . . . ?
 C4 Rh1 C1 C10 -157.2(3) . . . . ?
 C4 Rh1 C2 C1 -80.86(19) . . . . ?
 C4 Rh1 C2 C3 36.02(18) . . . . ?
 C4 Rh1 C2 C6 157.8(5) . . . . ?
 C4 Rh1 C3 C2 -119.1(3) . . . . ?
 C4 Rh1 C3 C7 122.6(5) . . . . ?
 C4 Rh1 C5 C1 118.3(3) . . . . ?
 C4 Rh1 C5 C9 -120.0(4) . . . . ?
 C4 Rh1 N1 C12 43.0(5) . . . . ?
 C5 C1 C2 C3 -0.8(3) . . . . ?
 C5 C1 C2 C6 -176.1(3) . . . . ?
 C5 C1 C2 Rh1 61.54(19) . . . . ?
 C5 C1 C10 C11 -69.6(5) . . . . ?
 C5 Rh1 C1 C2 117.5(3) . . . . ?
 C5 Rh1 C1 C10 -119.8(4) . . . . ?
 C5 Rh1 C2 C1 -37.87(17) . . . . ?
 C5 Rh1 C2 C3 79.01(19) . . . . ?
 C5 Rh1 C2 C6 -159.2(5) . . . . ?
 C5 Rh1 C3 C2 -81.89(19) . . . . ?
 C5 Rh1 C3 C4 37.24(18) . . . . ?
 C5 Rh1 C3 C7 159.9(5) . . . . ?
 C5 Rh1 C4 C3 -119.5(3) . . . . ?
 C5 Rh1 C4 C8 116.8(4) . . . . ?
 C5 Rh1 N1 C12 39.0(4) . . . . ?
 C6 C2 C3 C4 175.7(3) . . . . ?
 C6 C2 C3 C7 -2.8(5) . . . . ?
 C6 C2 C3 Rh1 -123.3(4) . . . . ?
 C7 C3 C4 C5 178.8(3) . . . . ?
 C7 C3 C4 C8 0.3(6) . . . . ?
 C7 C3 C4 Rh1 -122.4(4) . . . . ?
 C8 C4 C5 C1 177.7(3) . . . . ?
 C8 C4 C5 C9 2.8(5) . . . . ?
 C8 C4 C5 Rh1 -121.6(3) . . . . ?
 C10 C1 C2 C3 -179.3(3) . . . . ?
 C10 C1 C2 C6 5.4(5) . . . . ?
 C10 C1 C2 Rh1 -116.9(3) . . . . ?
 C10 C1 C5 C4 179.6(3) . . . . ?
 C10 C1 C5 C9 -5.8(5) . . . . ?
 C10 C1 C5 Rh1 117.5(3) . . . . ?
 C10 C11 C12 N1 75.1(6) . . . . ?
 N1 Rh1 C1 C2 -117.8(2) . . . . ?
 N1 Rh1 C1 C5 124.78(19) . . . . ?
 N1 Rh1 C1 C10 5.0(3) . . . . ?
 N1 Rh1 C2 C1 70.8(2) . . . . ?
 N1 Rh1 C2 C3 -172.27(18) . . . . ?
 N1 Rh1 C2 C6 -50.5(5) . . . . ?
 N1 Rh1 C3 C2 14.5(3) . . . . ?
 N1 Rh1 C3 C4 133.6(2) . . . . ?
 N1 Rh1 C3 C7 -103.7(5) . . . . ?
 N1 Rh1 C4 C3 -125.1(3) . . . . ?
 N1 Rh1 C4 C5 -5.7(4) . . . . ?
 N1 Rh1 C4 C8 111.1(4) . . . . ?
 N1 Rh1 C5 C1 -64.5(2) . . . . ?
 N1 Rh1 C5 C4 177.24(18) . . . . ?
 N1 Rh1 C5 C9 57.2(3) . . . . ?
 Cl1 Rh1 C1 C2 154.29(17) . . . . ?
 Cl1 Rh1 C1 C5 36.8(2) . . . . ?
 Cl1 Rh1 C1 C10 -82.9(3) . . . . ?
 Cl1 Rh1 C2 C1 -73.0(4) . . . . ?
 Cl1 Rh1 C2 C3 43.9(4) . . . . ?
 Cl1 Rh1 C2 C6 165.6(4) . . . . ?
 Cl1 Rh1 C3 C2 -163.32(15) . . . . ?
 Cl1 Rh1 C3 C4 -44.2(2) . . . . ?
 Cl1 Rh1 C3 C7 78.4(5) . . . . ?
 Cl1 Rh1 C4 C3 144.8(2) . . . . ?
 Cl1 Rh1 C4 C5 -95.72(17) . . . . ?
 Cl1 Rh1 C4 C8 21.0(4) . . . . ?
 Cl1 Rh1 C5 C1 -152.94(16) . . . . ?
 Cl1 Rh1 C5 C4 88.75(18) . . . . ?
 Cl1 Rh1 C5 C9 -31.3(3) . . . . ?
 Cl1 Rh1 N1 C12 135.3(3) . . . . ?
 Cl2 Rh1 C1 C2 -30.4(2) . . . . ?
 Cl2 Rh1 C1 C5 -147.82(14) . . . . ?
 Cl2 Rh1 C1 C10 92.4(3) . . . . ?
 Cl2 Rh1 C2 C1 159.02(16) . . . . ?
 Cl2 Rh1 C2 C3 -84.10(18) . . . . ?
 Cl2 Rh1 C2 C6 37.7(5) . . . . ?
 Cl2 Rh1 C3 C2 100.56(17) . . . . ?
 Cl2 Rh1 C3 C4 -140.31(19) . . . . ?
 Cl2 Rh1 C3 C7 -17.7(5) . . . . ?
 Cl2 Rh1 C4 C3 48.2(2) . . . . ?
 Cl2 Rh1 C4 C5 167.65(14) . . . . ?
 Cl2 Rh1 C4 C8 -75.6(4) . . . . ?
 Cl2 Rh1 C5 C1 88.9(3) . . . . ?
 Cl2 Rh1 C5 C4 -29.4(3) . . . . ?
 Cl2 Rh1 C5 C9 -149.5(3) . . . . ?
 Cl2 Rh1 N1 C12 -131.3(3) . . . . ?
 Rh1 C1 C2 C3 -62.4(2) . . . . ?
 Rh1 C1 C2 C6 122.3(3) . . . . ?
 Rh1 C1 C5 C4 62.1(2) . . . . ?
 Rh1 C1 C5 C9 -123.2(3) . . . . ?
 Rh1 C1 C10 C11 19.1(5) . . . . ?
 Rh1 C2 C3 C4 -61.0(2) . . . . ?
 Rh1 C2 C3 C7 120.5(3) . . . . ?
 Rh1 C3 C4 C5 -58.9(2) . . . . ?
 Rh1 C3 C4 C8 122.7(4) . . . . ?
 Rh1 C4 C5 C1 -60.72(19) . . . . ?
 Rh1 C4 C5 C9 124.4(3) . . . . ?
 Rh1 N1 C12 C11 -40.8(6) . . . . ?

_olex2_submission_special_instructions 'No special instructions were received'